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化学镀制备玄武岩纤维/镍核壳结构及其表征
康玉清,袁轩一,曹茂盛
北京理工大学材料科学与工程学院,北京100081
摘要:
采用简单易行的化学镀方法,在较低的温度下制备出一种新型的玄武岩纤维/镍核壳结构。SEM、XRD、XPS分析结果表明,金属Ni颗粒吸附在玄武岩纤维表面,形成了一层均匀连续的镍壳层。通过对试验结果进行分析,得出了制备玄武岩纤维/镍核壳结构的最佳温度和pH值分别为50℃和10.0。文中对化学镀核壳结构的形成机理也进行了初步分析。
关键词:  玄武岩纤维  核壳结构  化学镀
DOI:
分类号:
基金项目:国防科工委十一五基础科研计划(编号略 )和武器装备预研基金(编号略)资助课题。
Preparation and Characterization of Basalt Fibers/nickel core-shell Structures Synthesized by Electroless Plating
KANG Yu-Qing,YUAN Xuan-Yi,CAO Mao-Sheng
School of Material Science and Engineering, Beijing Institute of Technology, Beijing 100081 China
Abstract:
Basalt fibers/nickel core-shell structures were synthesized by an electroless plating method at low temperature. The core-shell structures were characterized by means of SEM and their components were analyzed by EDS, XRD and XPS. The results showed that the surface of basalt fibers was coated by a continuous and uniform nickel shells. Especially, the optimal temperature and pH value of electroless plating, namely, 50℃ and 10.0, have been ascertained. The possible mechanism of the formation of basalt fibers/nickel core-shell structures was discussed.
Key words:  basalt fibers  core-shell structures  electroless plating