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纳米微囊砂轮磨削工件表面自润滑层的形成
关集俱1, 徐正亚1, 杨兰玉1, 夏雨2, 许雪峰2
1.常熟理工学院机械工程学院 苏州 215500;2.浙江工业大学特种装备制造与先进加工技术教育部重点实验室 杭州 310014
摘要:
在磨削时磨削液难以有效渗入磨削区域起冷却润滑作用。提出利用润滑剂油酸(OA)填充碳纳米管(CNTs)制备 CNTs@OA 纳米微囊,并以其为填充剂制备树脂砂轮,磨削时随着纳米微囊的破裂,油酸可释放到磨削区形成自润滑层起润滑作用,从而提高砂轮的磨削性能。首先,制备纳米微囊并对其进行表征,分析微囊在砂轮中的存在形式,考察微囊的填充对其力学性能的影响;其次,研究砂轮磨削 GCr15 钢时纳米微囊的含量和磨削速度对磨削力、磨削温度、磨削比和表面粗糙度的影响,分析磨削过程中纳米微囊释放润滑剂油酸并产生自润滑作用的机制。结果表明,纳米微囊具有较好的热稳定性, 能够抵抗树脂砂轮的固化温度并保护其中的油酸,当微囊的填充量小于 16%时,砂轮的力学性能可以满足使用需求。与普通砂轮比,纳米微囊砂轮磨削时的磨削力可减小 40%,磨削温度降低 45%,工件表面粗糙度减少 15%,磨削比可提高 30%。磨削过程中,砂轮中的纳米微囊可将其空腔中的润滑剂油酸不断被释放到磨削界面上形成自润滑层,使砂轮具有了较好的自润滑作用,从而提高了其磨削性能。研究成果可为解决磨削过程的润滑问题提供一种可行的技术路线。
关键词:  碳纳米管  油酸  纳米微囊  砂轮  自润滑  磨削性能
DOI:10.11933/j.issn.1007-9289.20230214002
分类号:TH162
基金项目:国家自然科学基金(51805345,52275468)
Formation of Self-lubricating Layer on Workpiece Surface Ground by Nano-encapsulated Grinding Wheel
GUAN Jiju1, XU Zhengya1, YANG Lanyu1, XIA Yu2, XU Xuefeng2
1.College of Mechanical Engineering, Changshu Institute of Technology, Soochow 215500 , China;2.Key Laboratory of Special Purpose Equipment and Advanced Manufacturing Technology ofMinistry of Education, Zhejiang University of Technology, Hangzhou 310014 , China
Abstract:
Among the many machining methods available, grinding is one of the most important and is primarily used for the final processing of different machine parts. The grinding wheel rotates at a high speed, which creates an airflow barrier around the grinding area, preventing the grinding fluid from effectively cooling and lubricating the area during grinding. This leads to grinding burns and other surface quality problems of the workpiece and affects machining efficiency. To address this problem, this study proposes filling the cavity of carbon nanotubes (CNTs) with an oleic acid (OA) lubricant, which is used as a filler in resin-bonded grinding wheels. Using this nano-capsule as a filler could help improve the strength of the grinding wheel owing to the high strength and thermal stability of the CNTs. The most important benefit of this method is the release of oleic acid into the grinding area when the nano-capsules rupture, and the self-lubricating layer formed can directly lubricate the grinding area, thereby improving the performance of the grinding wheel. First, nano-capsules are prepared by widely used wet chemical methods and then characterized by Thermogravimetric Analysis (TG), Fourier Transform Infrared Spectroscopy (FTIR), and Transmission Electron Microscopy (TEM)to evaluate the material stability, surface functional groups, and morphology. In addition, we evaluate the presence of nano-capsules in the grinding wheel and the effect of the nano-capsule filling on the tensile strength and hardness of the grinding wheel. Finally, the effects of the nano-capsule content and grinding speed on the grinding force, grinding temperature, grinding ratio, and workpiece surface roughness during the grinding of GCr15 steel are studied. The release of OA in the grinding wheel during the grinding process is studied using X-ray photoelectron spectroscopy and scanning electron microscopy (SEM) analysis of the workpiece surface, based on which the formation mechanism of the self-lubricating film is further clarified. A mechanism for the lubrication effect of the self-lubricating film is also proposed. The nano-capsules were successfully prepared by wet chemical methods; they were found to have a filling rate of approximately 20% and were thermally stable. During the curing process, the nano-capsules could resist the curing temperature of the resin and effectively protect the oleic acid. According to the tensile test, the nano-capsules increased the strength of the grinding wheel by approximately 25% when the filling amount was approximately 8%. Further filling of the nano-capsules reduced the tensile strength of the grinding wheel, and the hardness of the grinding wheel continued to decrease with an increase in the nano-capsule content. Moreover, the mechanical properties of the grinding wheel satisfied the requirements of its intended use when the nano-capsule filling content was less than 16%. Compared with ordinary resin grinding wheels, the grinding force of the nano-capsule filled grinding wheels can be reduced by 40%, the grinding temperature can be reduced by 45%, the surface roughness value can be reduced by 15%, and the grinding ratio can be increased by 30%. The nano-capsules embedded in the grinding wheel continuously released OA within its cavity onto the grinding interface during the surface grinding process, forming a composite self-lubricating layer. Because of this lubricating layer, the grinding wheel achieved better lubrication performance, which in turn improves the grinding performance of the wheel. The research presented in this paper provides a viable technical solution for grinding lubrication problems, which is beneficial for improving the grinding efficiency and surface quality of workpieces. The grinding wheel developed in this study has significant potential for application in green machining conditions where a large amount of grinding fluid is not allowed.
Key words:  carbon nanotubes  oleic acid  nano-capsules  grinding wheel  self-lubricating  grinding performance