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20CrNiMo表面针状空心阴极辉光放电制备TiN研究
陈 飞,赫 单,陈家庆,周 海
北京石油化工学院 工程教育中心
摘要:
在真空炉内以针状钛丝为溅射源极,以氩气和氮气为放电气体,利用辉光放电现象、尖端放电和空心阴极效应在20CrNiMo表面复合渗镀合成TiN改性层,目的是提高20CrNiMo表面的耐磨性能。利用扫描电子显微镜(SEM)观察了改性层的截面形貌;测量了改性层的显微硬度并用XRD观察分析了改性层的相结构;采用MFT–4000型高速往复磨损试验机对渗镀改性层的摩擦磨损性能进行了研究。结果表明:在试验工艺条件下20CrNiMo试样表面制备的TiN改性层厚度约为40 μm。改性后表面摩擦因数为0.169,较20CrNiMo基体的摩擦因数0.324明显减小,耐磨性能提高。
关键词:  TiN改性层  辉光放电  针状空心阴极  耐磨性
DOI:
分类号:
基金项目:国家自然基金项目(50874018)
Study on the TiN Modified Layer on the Surface of 20CrNiMo Steel by Needle–shape Cathode Glow Discharging
CHEN Fei, HE Dan, CHEN Jia–qing, ZHOU Hai
Engineering Education Center, Beijing Institute of Petrochemical Technology
Abstract:
The multiple structures made of alloying and coating layers of TiN was achieved on the surface of 20CrNiMo steel by the needle–shape cathode glow discharging. It is aimed to reduce the friction coefficient of the 20CrNiMo and to improve the property of the wear–resistance. The morphology of TiN modified layer at the cross section was observed by Scanning Electron Microscope (SEM). The friction and wear behavior of the TiN/ZrN films under dry sliding against GCr15 steel was evaluated on a MFT–4000 high speed to–and–fro wear test rig. The results showed that it was feasible to prepare TiN layer of 40 μm thickness by the needle–shape cathode glow discharging. It has been found that the TiN modified layer has excellent friction and wear–resistant behaviors. The friction coefficient of the 20CrNiMo substrate was about 0.324 under dry sliding, while the TiN modified layer experienced much abated friction coefficient to 0.169 under the same testing condition.
Key words:  TiN modified layer  cathode glow discharge  wear–resistance behavior