引用本文:顾艳红， 马慧娟， 陈玲玲， 杨远航， 刘琦， 刘家浚.Ti6Al4V钛合金超声波冷锻/微弧氧化涂层的制备及耐磨性能[J].中国表面工程,2016,29(1):87~95
GU Yanhong, MA Huijuan, CHEN Lingling, YANG Yuanhang, LIU Qi, LIU Jiajun.Wear Resistance of MAO Coated Ti6Al4V Alloy Prepared by Ultrasonic Cold Forging Technology[J].China Surface Engineering,2016,29(1):87~95
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Ti6Al4V钛合金超声波冷锻/微弧氧化涂层的制备及耐磨性能
顾艳红， 马慧娟， 陈玲玲， 杨远航， 刘琦， 刘家浚1,2,3
1. 北京石油化工学院 机械工程学院, 北京 102617;2. 北京化工大学 机电工程学院, 北京 100029;3. 清华大学 机械工程系, 北京 100084
摘要:
为了提高生物医用钛合金的耐磨性，利用超声波冷锻技术（UCFT）作为预处理，采用微弧氧化（MAO）技术制备出具有生物活性的MAO涂层。采用透射电子显微镜(TEM)和原子力显微镜(AFM)测量钛合金UCFT处理后表面纳米晶粒大小和表面粗糙度，采用扫描电子显微镜(SEM)、X射线衍射仪(XRD)和显微硬度计测量涂层的微观形貌、相组成和显微硬度，并在高速往复摩擦磨损试验机上对试样进行摩擦学性能测试。结果表明：超声波冷锻后的钛合金表面晶粒得到细化，平均表面粗糙度仅为36.98 nm；UCFTMAO涂层的显微硬度从330 HV0.05提高到518 HV0.05, 经超声波冷锻预处理后的微弧氧化涂层的摩擦因数降低，UCFTMAO试样在仿生液中的磨损量仅为基体试样的1/3。超声波冷锻技术作为预处理，显著提高了钛合金微弧氧化涂层的耐磨性能。
关键词:  钛合金  超声波冷锻  微弧氧化  耐磨性
DOI：10.11933/j.issn.1007-9289.2016.01.013
分类号:
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Wear Resistance of MAO Coated Ti6Al4V Alloy Prepared by Ultrasonic Cold Forging Technology
GU Yanhong, MA Huijuan, CHEN Lingling, YANG Yuanhang, LIU Qi, LIU Jiajun1,2,3
1. College of Mechanical Engineering, Beijing Institute of Petrochemical Technology, Beijing 102617;2.College of Mechanical and Electrical Engineering, Beijing University of Chemical Technology, Beijing 100029;3. Department of Mechanical Engineering, Tsinghua University, Beijing 100084
Abstract:
To improve the wear resistance of biomedical titanium alloys, ultrasound cold forging technology (UCFT) was used as a pretreatment before microarc oxidation (MAO) coatings were prepared. The grain size and surface roughness of the sample treated by UCFT was measured by transmission electron microscope (TEM) and atomic force microscope (AFM). Morphologies and phase composition were conducted by scan electron microscope (SEM) and Xray diffraction (XRD). Microhardness tester was used to measure the sample hardness. The highspeed reciprocating friction and wear tester was used to test the wear performance of the samples. The results show that the surface of titanium alloys is refined with small grain by UCFT. The average surface roughness is only 36.98 nm. The hardness increases from 330 HV0.05 of the untreated samples to 518 HV0.05 of the UCFTMAO samples. The friction coefficient decreases and the weight loss of impreved by UCFTMAO samples is only one third of the untreated samples. The wear resistance of the MAO coated titanium alloys is improved by UCFT processing.
Key words:  titanium alloys  ultrasonic cold forging technology (UCFT)  microarc oxidation（MAO）  wear resistance
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