引用本文:李静楠, 郭丹, 王元元.基于原子力显微镜的纳米抛光颗粒的摩擦力测量方法[J].中国表面工程,2012,25(2):21~25
LI Jing-nan, GUO Dan, WANG Yuan-yuan.Measurement of Interfacial Friction Force of Nanoparticles by Atomic Force Microscope[J].China Surface Engineering,2012,25(2):21~25
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基于原子力显微镜的纳米抛光颗粒的摩擦力测量方法
李静楠, 郭丹, 王元元
清华大学 摩擦学国家重点实验室, 北京 100084
摘要:
基于原子力显微镜接触模式,使用侧向力扫描测量单个纳米颗粒与基底表面的摩擦力,从而为颗粒从基底表面去除提供最为直接的测试方法。对硅片表面进行羟基化增强其亲水性,将聚苯乙烯纳米颗粒单层均匀地分散到硅片上。使用横向力模式和NanoMan两种方法侧向推动纳米颗粒,测得单个颗粒与硅片表面之间的最大静摩擦力分别为(1.57±0.09) μN和(1.51±0.13) μN,试验结果基本一致,表明这两种测量方法可靠有效。此外,NanoMan可控制针尖推动单个颗粒在基底表面做滑移运动,表明颗粒基底的滑动摩擦力与针尖施加载荷和扫描速度密切相关。
关键词:  原子力显微镜  纳米颗粒  摩擦力  横向力模式  NanoMan
DOI:
分类号:
基金项目:国家自然科学基金(91023016);国家973计划(2009CB724201)
Measurement of Interfacial Friction Force of Nanoparticles by Atomic Force Microscope
LI Jing-nan, GUO Dan, WANG Yuan-yuan
State Key Laboratory of Tribology, Tsinghua University, Beijing 100084
Abstract:
Measuring the friction force during the lateral manipulation of individual nanoparticle with the atomic force microscope technique is a straightforward approach to evaluate the removal of nanoparticles from the substrate. The silicon wafer was hydroxylated to enhance the hydrophilic property, and then diluted polystyrene latex was deposited on the wafer to form a dispersive singlelayer. Both atomic force microscope / lateral force mode and atomic force microscope /NanoMan modes were used to push the individual particle laterally, and the maximum static friction forces were (1.57±0.09) μN and (1.51±0.13) μN, respectively. The results show that the two methods are reliable and effective. In addition, the NanoMan mode was used to push individual nanoparticle to slide along a given path. The results indicate that the sliding friction force between nanoparticles and substrate closely correlate with applied load and velocity of the tip.
Key words:  atomic force microscope(AFM)  nanoparticles  friction force  lateral force mode(LFM)  NanoMan mode
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